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When the 1V-LSD hemitartrate salt was subjected to basification and extraction with diethyl ether just before GC-MS Investigation, it had been found that hydrolysis to LSD happened (Supporting Data). Additionally, three extra 1V-LSD isomers ended up detected while in the GC-MS TIC trace with 1V-LSD labeled as isomer I. When the 1V-LSD salt was diss